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Purity:99%
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Uses |
It is an intermediate in organic syntheses and used as a pharmaceutical intermediates. |
Cyanobacteria Synechocystis sp. PCC 6803...
Most ligands applied for asymmetric hydr...
Enantiopure secondary alcohols are funda...
The invention discloses a tridentate nit...
2-chlorostyrene
(S)-1-(2'-chlorophenyl)ethanol
2-(2-chlorophenyl)-1-ethanol
(R)-1-(o-chlorophenyl)ethanol
| Conditions | Yield |
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2-chlorostyrene; With benzo[1,3,2]dioxaborole; rhodium complex 8; In toluene; at 20 ℃; for 2h;
With sodium hydroxide; water; dihydrogen peroxide; In toluene; at 20 ℃; for 2h; Title compound not separated from byproducts;
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2-chlorostyrene; With bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; (1R,2R)-1,2-bis(di[2-furyl]phosphanyl)cyclohexane; benzo[1,3,2]dioxaborole; In 1,2-dimethoxyethane; toluene; at -75 ℃; for 1h;
With potassium hydroxide; dihydrogen peroxide; In 1,2-dimethoxyethane; Title compound not separated from byproducts;
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With pinacol borane; 4 A molecular sieve; Rh(2,5-norbornadiene)2BF4; In 1,2-dimethoxyethane; at 20 ℃; for 12h; Title compound not separated from byproducts.;
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2-chlorostyrene
(S)-1-(2'-chlorophenyl)ethanol
2-(2-chlorophenyl)-1-ethanol
(R)-1-(o-chlorophenyl)ethanol
| Conditions | Yield |
|---|---|
|
2-chlorostyrene; With benzo[1,3,2]dioxaborole; rhodium complex 8; In toluene; at 20 ℃; for 2h;
With sodium hydroxide; water; dihydrogen peroxide; In toluene; at 20 ℃; for 2h; Title compound not separated from byproducts;
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2-chlorostyrene; With bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; (1R,2R)-1,2-bis(di[2-furyl]phosphanyl)cyclohexane; benzo[1,3,2]dioxaborole; In 1,2-dimethoxyethane; toluene; at -75 ℃; for 1h;
With potassium hydroxide; dihydrogen peroxide; In 1,2-dimethoxyethane; Title compound not separated from byproducts;
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With pinacol borane; 4 A molecular sieve; Rh(2,5-norbornadiene)2BF4; In 1,2-dimethoxyethane; at 20 ℃; for 12h; Title compound not separated from byproducts.;
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1-(2-chlorophenyl)ethanone
2-chlorostyrene
vinyl acetate
2'-chloro-sec-phenethyl alcohol
2-propen-1-yl 1-{4-{[(1R)-1-(2-chlorophenyl)ethyl]oxy}-5-[(methyloxy)carbonyl]-2-thienyl}-1H-benzimidazole-5-carboxylate
methyl 5-(5-bromo-1H-benzimidazol-1-yl)-3-{[(1R)-1-(2-chlorophenyl)ethyl]oxy}thiophene-2-carboxylate
C21H16BrClN2O3S
5-(5-bromo-1H-benzimidazol-1-yl)-3-({(1R)-1-[2-chlorophenyl]ethyl}oxy)thiophene-2-carboxamide